Preparation of aluminum nitride from poly (isopropyliminoalane)

Yoshiyuki Sugahara; Tsutomu Onuma; Osamu Tanegashima; Kazuyuki Kuroda; Chuzo Kato

doi:10.2109/jcersj.100.101

Preparation of aluminum nitride from poly (isopropyliminoalane)

Yoshiyuki Sugahara^*, Tsutomu Onuma, Osamu Tanegashima, Kazuyuki Kuroda, Chuzo Kato

^*Corresponding author for this work

School of Advanced Science and Engineering

Research output: Contribution to journal › Article › peer-review

19 Citations (Scopus)

Abstract

Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state ²⁷Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.

Original language	English
Pages (from-to)	101-103
Number of pages	3
Journal	Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
Volume	100
Issue number	1157
DOIs	https://doi.org/10.2109/jcersj.100.101
Publication status	Published - 1992

ASJC Scopus subject areas

Ceramics and Composites
Chemistry(all)
Condensed Matter Physics
Materials Chemistry

Access to Document

10.2109/jcersj.100.101

Cite this

@article{36860c8d1a594f6884aa8fce8c90c18a,

title = "Preparation of aluminum nitride from poly (isopropyliminoalane)",

abstract = "Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state 27Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.",

author = "Yoshiyuki Sugahara and Tsutomu Onuma and Osamu Tanegashima and Kazuyuki Kuroda and Chuzo Kato",

year = "1992",

doi = "10.2109/jcersj.100.101",

language = "English",

volume = "100",

pages = "101--103",

journal = "Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan",

issn = "1882-0743",

publisher = "Ceramic Society of Japan/Nippon Seramikkusu Kyokai",

number = "1157",

}

TY - JOUR

T1 - Preparation of aluminum nitride from poly (isopropyliminoalane)

AU - Sugahara, Yoshiyuki

AU - Onuma, Tsutomu

AU - Tanegashima, Osamu

AU - Kuroda, Kazuyuki

AU - Kato, Chuzo

PY - 1992

Y1 - 1992

N2 - Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state 27Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.

AB - Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state 27Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.

UR - http://www.scopus.com/inward/record.url?scp=0026746795&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0026746795&partnerID=8YFLogxK

U2 - 10.2109/jcersj.100.101

DO - 10.2109/jcersj.100.101

M3 - Article

AN - SCOPUS:0026746795

SN - 1882-0743

VL - 100

SP - 101

EP - 103

JO - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan

JF - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan

IS - 1157

ER -

Preparation of aluminum nitride from poly (isopropyliminoalane)

Abstract

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this