Transmission electron microscopic study on electroless plated nickel-molybdenum-phosphorus alloy film

Tetsuya Osaka, Katsuya Arai, Yohtaro Yamazaki, Tatsuru Namikawa

Research output: Contribution to journalArticlepeer-review

3 Citations (Scopus)

Abstract

In order to clarify the cause of the particular annealing behavior of resistivity of electroless Ni–Mo–P alloy films, the film structure after various heat treatment of a typical crystalline Ni-Mo-P alloy film by electroless plating was investigated by transmission electron microscopy (TEM). In the Ni–Mo–P film under as-plated conditions, the lattice image is observed, but it contains some regions having no lattice images due to amorphous conditions. The structure of small grains is kept even after heat treatment at 400°C, but the nonuniformity of Mo concentration is confirmed to exist in the film. After heat treatment at 700°C, the grains become larger and crystals with complete lattice images and no defects are observed. The results support the annealing effect of resistivity of the crystalline Ni–Mo–P alloy film, which shows a maximum upon heat treatment at around 400–500°C.

Original languageEnglish
Pages (from-to)229-233
Number of pages5
JournalJapanese journal of applied physics
Volume28
Issue number2 R
DOIs
Publication statusPublished - 1989 Feb

Keywords

  • Annealing effect
  • Electroless plating
  • Microstructure
  • Nickle-molybdenum alloy
  • Transmission electron microscopy

ASJC Scopus subject areas

  • Engineering(all)
  • Physics and Astronomy(all)

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