Catalytic Dearomative Spirocyclization via Gold Carbene Species Derived from Ynamides: Efficient Synthesis of 2-Azaspiro[4.5]decan-3-ones

Mamoru Ito, Ryosuke Kawasaki, Kyalo Stephen Kanyiva, Takanori Shibata*

*この研究の対応する著者

研究成果: Article査読

16 被引用数 (Scopus)

抄録

An intramolecular catalytic dearomatization of phenols via gold carbene species proceeded to provide 2-azaspiro[4.5]decan-3-ones. The use of NHC ligand and water as a co-solvent was critical for achieving high reactivity. This reaction did not require hazardous diazo compounds as carbene sources and proceeded even under air. The obtained spirocyclic product could be readily transformed into a gabapentin derivative by hydrogenation and deprotection.

本文言語English
ページ(範囲)3721-3724
ページ数4
ジャーナルChemistry - A European Journal
24
15
DOI
出版ステータスPublished - 2018 3月 12

ASJC Scopus subject areas

  • 触媒
  • 有機化学

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