TY - JOUR
T1 - Crystal structure of a methanesulfonate salt of 4-(N-methyl)pyridinium boronic acid
AU - Iwatsuki, Satoshi
AU - Kanamitsu, Yuki
AU - Ohara, Hidetaka
AU - Kawahata, Masatoshi
AU - Danjo, Hiroshi
AU - Ishihara, Koji
PY - 2012
Y1 - 2012
N2 - The structure of a methanesulfonate salt of 4-(N-methyl)pyridinium boronic acid, [4-(N-Me)PyB(OH)2]CH3SO3·H2O, was determined by X-ray crystallography, and was characterized as: P1, a = 5.6937(16), b = 7.805(2), c = 13.522(3)Å, α = 99.46(3), β = 91.45(3), γ = 108.014(17)°, Z = 2, V = 561.8(2)Å3. In the crystals, the cation and the anion are linked by BOH·O(anion), BOH···O(water), and (water)OH···O(anion) hydrogen bonds to stabilize the 1:1:1-cation:anion:water salt unit.
AB - The structure of a methanesulfonate salt of 4-(N-methyl)pyridinium boronic acid, [4-(N-Me)PyB(OH)2]CH3SO3·H2O, was determined by X-ray crystallography, and was characterized as: P1, a = 5.6937(16), b = 7.805(2), c = 13.522(3)Å, α = 99.46(3), β = 91.45(3), γ = 108.014(17)°, Z = 2, V = 561.8(2)Å3. In the crystals, the cation and the anion are linked by BOH·O(anion), BOH···O(water), and (water)OH···O(anion) hydrogen bonds to stabilize the 1:1:1-cation:anion:water salt unit.
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U2 - 10.2116/xraystruct.28.63
DO - 10.2116/xraystruct.28.63
M3 - Article
AN - SCOPUS:84866764425
SN - 1883-3578
VL - 28
SP - 63
EP - 64
JO - X-ray Structure Analysis Online
JF - X-ray Structure Analysis Online
IS - 8
ER -