TY - JOUR
T1 - Microstructures and mechanical properties of fiber textures forming mesoscale structure of drawn fine high carbon steel wire
AU - Gondo, Shiori
AU - Tanemura, Rena
AU - Suzuki, Shinsuke
AU - Kajino, Satoshi
AU - Asakawa, Motoo
AU - Takemoto, Kosuke
AU - Tashima, Kenichi
N1 - Funding Information:
This work was supported by Japan Society for the Promotion of Science (JSPS) Grant-in-Aid for JSPS Research Fellow Grant Number 16J11098 and was partly executed under the cooperation of organization between Waseda University and JXTG Nippon Oil & Energy Corporation. We also express gratitude to Nippon Steel & Sumikin SG Wire Co., Ltd. for providing materials. We appreciate the help received from Prof. K. Yoshida of Tokai University and Dr. T. Shinohara of Tanaka Kikinzoku Kogyo K. K. with measuring the electric resistivity. We also wish to acknowledge valuable discussions about crystal orientation with Prof. N. Nakada of Tokyo Institute of Technology.
Funding Information:
This work was supported by Japan Society for the Promotion of Science (JSPS) Grant-in-Aid for JSPS Research Fellow Grant Number 16J11098 and was partly executed under the cooperation of organization between Waseda University and JXTG Nippon Oil & Energy Corporation. We also express gratitude to Nippon Steel & Sumikin SG Wire Co., Ltd. for providing materials. We appreciate the help received from Prof. K. Yoshida of Tokai University and Dr. T. Shinohara of Tanaka Kikinzoku Kogyo K. K. with measuring the electric resistivity. We also wish to acknowledge valuable discussions about crystal orientation with Prof. N. Nakada of Tokyo Institute of Technology.
Publisher Copyright:
© 2018 Elsevier B.V.
PY - 2019/2/18
Y1 - 2019/2/18
N2 - The crystal orientation of a drawn high carbon steel wire was analyzed through electron backscatter diffraction analysis under the assumption that the wire consists of a mesoscale structure characterized by the fiber texture. The microstructure forming the mesoscale structure and the mechanical properties depending on the mesoscale structure were explained by the results of transmission electron microscopy observation, measurement of the electrical resistivity, differential scanning calorimetry thermal analysis, and tensile testing. In the beginning of the wire drawing, the wire has only {100}<110>−{111}<110> (the primary fiber texture). Then, the wire has this orientation at the outer side and {110}<110>−{111}<110> (the secondary fiber texture) at the inner side. At a drawing strain larger than approximately 2.7, the subprimary fiber texture ({100}<110>−{111}<110>) is formed at the outer side and will occupy the volume of the wire. The results indicate that with the increase of the drawing strain, the lamellar spacing decreased, and the amount of lattice defects increased. The tensile strength, uniform elongation, and reduction of area were typically uniform in the radial direction of the wire. On the other hand, the wire with only the primary fiber texture had lamellae whose angle with respect to the drawing direction decreased during wire drawing, as well as a surface layer with low longitudinal ductility. The wire with the subprimary fiber texture contained decomposed cementite. The wire also had a large variation of reduction of area. Increasing the back stress ratio shifts the transition of the mesoscale structure to a lower drawing strain.
AB - The crystal orientation of a drawn high carbon steel wire was analyzed through electron backscatter diffraction analysis under the assumption that the wire consists of a mesoscale structure characterized by the fiber texture. The microstructure forming the mesoscale structure and the mechanical properties depending on the mesoscale structure were explained by the results of transmission electron microscopy observation, measurement of the electrical resistivity, differential scanning calorimetry thermal analysis, and tensile testing. In the beginning of the wire drawing, the wire has only {100}<110>−{111}<110> (the primary fiber texture). Then, the wire has this orientation at the outer side and {110}<110>−{111}<110> (the secondary fiber texture) at the inner side. At a drawing strain larger than approximately 2.7, the subprimary fiber texture ({100}<110>−{111}<110>) is formed at the outer side and will occupy the volume of the wire. The results indicate that with the increase of the drawing strain, the lamellar spacing decreased, and the amount of lattice defects increased. The tensile strength, uniform elongation, and reduction of area were typically uniform in the radial direction of the wire. On the other hand, the wire with only the primary fiber texture had lamellae whose angle with respect to the drawing direction decreased during wire drawing, as well as a surface layer with low longitudinal ductility. The wire with the subprimary fiber texture contained decomposed cementite. The wire also had a large variation of reduction of area. Increasing the back stress ratio shifts the transition of the mesoscale structure to a lower drawing strain.
KW - Crystal orientation
KW - DSC thermal analysis
KW - EBSD analysis
KW - Ferrite
KW - Fiber texture
KW - High carbon steel wire
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U2 - 10.1016/j.msea.2018.11.121
DO - 10.1016/j.msea.2018.11.121
M3 - Article
AN - SCOPUS:85060338329
SN - 0921-5093
VL - 747
SP - 255
EP - 264
JO - Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing
JF - Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing
ER -