Preparation of aluminum nitride from poly (isopropyliminoalane)

Yoshiyuki Sugahara; Tsutomu Onuma; Osamu Tanegashima; Kazuyuki Kuroda; Chuzo Kato

doi:10.2109/jcersj.100.101

Preparation of aluminum nitride from poly (isopropyliminoalane)

Yoshiyuki Sugahara^*, Tsutomu Onuma, Osamu Tanegashima, Kazuyuki Kuroda, Chuzo Kato

^*この研究の対応する著者

先進理工学部

研究成果: Article › 査読

19 被引用数 (Scopus)

抄録

Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state ²⁷Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.

本文言語	English
ページ（範囲）	101-103
ページ数	3
ジャーナル	Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
巻	100
号	1157
DOI	https://doi.org/10.2109/jcersj.100.101
出版ステータス	Published - 1992

ASJC Scopus subject areas

セラミックおよび複合材料
化学 (全般)
凝縮系物理学
材料化学

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10.2109/jcersj.100.101

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AU - Sugahara, Yoshiyuki

AU - Onuma, Tsutomu

AU - Tanegashima, Osamu

AU - Kuroda, Kazuyuki

AU - Kato, Chuzo

PY - 1992

Y1 - 1992

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AB - Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state 27Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.

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Preparation of aluminum nitride from poly (isopropyliminoalane)

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